5,10,15,20-四(4-磺酸基-苯基)卟啉合成的方法研究
The Synthesis Method for 5, 10, 15, 20 tetra (p-sulfonato) Phenylporphyrin

王伟军 WWJ

摘要


用2种方法合成了5,10,15,20-四(磺酸基-苯基)卟啉,实验表明:用氯仿作溶剂,氯磺酸作磺化剂比浓硫酸环境中磺化制备有明显的高的产率,且反应时间短、操作条件也相对简单.
In this research, two methods were used to synthesize the 5, 10, 15, 20tetra(p-sulfonato) Phenylporphyrin. Experimental results showed that the 5, 10, 15, 20tetra(p-sulfonato) Phenylporphyrin synthesized has a higher yield in terms of the reaction of chlorosulfonato acid in CHCl3 than sulfonato (the reagent was the condensed sulfonato acid), and the time is short and the operation is easy.

参考



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